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Synthesis, Characterization and Thermal Properties of Some New Azopolyimides
几种新型偶氮聚酰亚胺的合成、表征及热性能
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Synthesis, characterization and thermal properties of some new azopolyimides By: Logesh, G.; et al Asian Journal of Chemistry (2012), 24(7), 3033-3038 A new class of aromatic azopolyimides were synthesized from aromatic diamine with 3,3',4,4'-azobenzenetetracarboxlic dianhydride. The synthesis involved the reaction of the dianhydride with resp. diamine to yield an intermediate, soluble, open chain precursor polymer of polyamic acid, which on further cyclodehydration by solution, chem. and thermal imidization method yielded the less soluble, high viscosity, high stability, heat resistant or high temperature polyimides. All these polyimides were characterized by UV and IR. Viscosity, solubility, stability and thermal properties of these polymers were also studied. |
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