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 Scandium Metal–Organic Frameworks Containing Tetracarboxylate Linker Molecules: Synthesis, Structural Relationships, and Properties 相关领域
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结晶学
分子
金属有机骨架
发光
化学
溶剂热合成
晶体结构
八面体
立体化学
材料科学
有机化学
光电子学
吸附
计算机科学
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| 其它 | Three structurally related metal–organic frameworks (MOFs) of composition [Sc2(OH)2(L)] denoted Sc-CAU-9-PTCDA, Sc-CAU-9-TCPB, and Sc-CAU-9-H2TCPP containing the tetratopic linker molecules L14– = PTCDA4– (perylene-3,4,9,10-tetracarboxylate), L24– = TCPB4– (1,2,4,5-tetrakis(4-carboxylatophenyl)-benzene), or L34– = H2TCPP4– (meso-tetra(4-carboxylatophenyl)-porphyrin), have been obtained from solvothermal syntheses. The crystal structures were determined from powder X-ray diffraction data. The title compounds contain chains of trans corner-sharing [ScO6] octahedra, connected by the linker molecules to form three-dimensional networks. Depending on the shape of the respective linker the compounds crystallize in a frz or fry topology and with increasing size of the linker, an expansion of the framework and the formation of accessible channels are observed. |
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