Advances in Microencapsulation of Flavor Substances: Preparation Techniques, Wall Material Selection, Characterization Methods, and Applications

This review systematically examines advances in flavor microencapsulation technology from 2014 to 2024, focusing on innovations in preparation techniques, trends in wall material selection, and characterization methods. Literature metrological analysis shows that spray drying is the predominant technology (25% of reports); its shortcomings in volatile flavor retention have driven improved strategies such as vacuum low-temperature drying, ultrasound assistance, and monodisperse atomization. Emerging technologies such as electrohydrodynamic methods (electrospinning/electrospraying) and supercritical fluid processing are favored due to their nonthermal advantages. Overall, traditional polysaccharides have been widely used due to their good emulsifying and stabilizing properties. In the meanwhile, plant-based polysaccharides (e.g., inulin, hemicellulose) and proteins (e.g., pea protein) are increasingly preferred as the wall materials driven by sustainability and clean-labeling requirements. Morphological analysis and particle size and distribution studies have highlighted the key role of microstructure in stability and release kinetics, with multicore and multishell structures optimizing controlled release performance. Despite progress, gaps remain in the standardized assessment of encapsulation efficacy, the cost-effectiveness of novel materials, and practical food applications. In the future, a combination of interdisciplinary approaches is needed to investigate low-energy preparation technologies, functionalized wall materials, and intelligent release mechanisms to achieve the better application of flavor microencapsulates in food.