模拟体液
磷灰石
坐滴法
钙
钛
腐蚀
微观结构
磷酸盐
复合材料
X射线光电子能谱
表面改性
作者
Ekaterina G. Komarova,V. V. Chebodaeva,Yuriy P. Sharkeev,Maria Sedelnikova
出处
期刊:Key Engineering Materials
日期:2016-02-01
卷期号:683: 370-376
被引量:9
标识
DOI:10.4028/www.scientific.net/kem.683.370
摘要
The influence of the microarc oxidation parameters as electrical voltage and process duration on the surface morphology and topography, wettability and chemical composition of calcium phosphate coatings on the low elastic module Ti-40mas.%Nb (Ti-40Nb) alloy surface has been investigated. The linear growth of thickness and roughness and the linear decrease of the free surface energy with increasing process electrical voltage have been obtained. It was shown that calcium phosphate coatings have low contact angle with liquids and high free surface energy, as a consequence. It indicates a high hydrophilicity. X-ray diffraction analyses showed that the coatings after deposition have X-ray amorphous state that indicates high rate of coating dissolution. The coatings have maximum Ca/P ratio is 0.6. The optimal range of the oxidation voltage from 200 to 250 V and process duration from 5 to 10 min has been found. Such parameters allow to form the coating with the specific morphology, roughness and thickness and high hydrophylicity.
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