Aryl iodides smoothly react with NaN3 and CO in the presence of a Pd/Xantphos catalyst to give aroyl azides (ArCON3) in 75–92 % yield. The reaction occurs under mild reaction conditions (1 atm, 20–50 °C) and exhibits high functional-group tolerance. (Xantphos=9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene)
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(2025-6-4)
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