Dependence of deformation mechanisms on micro-pores in the fourth-generation single crystal superalloy during out-of-phase thermal-mechanical fatigue

The high-temperature and long-term solution heat treatments of fourth-generation single crystal (SX) superalloys have sparked an increasing number of homogenization pores in the alloy. Out-of-phase (OP) thermal-mechanical fatigue (TMF) experiments were conducted to elucidate the effect of pores on the fatigue behaviors and deformation mechanisms. The results showed that the plastic deformation was mainly concentrated upon γ matrix in regions away from pores, more specifically, intrinsic stacking fault (ISF) and extrinsic stacking fault (ESF) as well as dislocation cross-slipping were detected. In areas near micro-pores, however, the γ/γ′-structure was subjected to severe twinning shearing. High-resolution observation illustrated that the amount of ESF and a/6<112> twinning dislocations had remarkably increased. Besides, the partial dislocations were more prone to move in different slipping systems at these regions with considerable stress concentration. These factors collectively enabled the formation of deformation twins from the edge of micro-pores. Moreover, the twinning nucleation could occur near both H-pores and S-pores, while the increasing pore size would enhance the nucleation and propagation of pore-induced twins by a large margin. These findings reported have provided important guidance for the future application of the fourth-generation SX superalloys.