材料科学
立方氧化锆
多孔性
扫描电子显微镜
微观结构
烧结
复合材料
抗压强度
碳纳米管
弹性模量
陶瓷
作者
Bruno Henriques,Douglas Fabris,Elvira Lopes,Anderson Camargo Moreira,Iara Frangiotti Mantovani,Celso Peres Fernandes,Márcio C. Fredel
标识
DOI:10.1002/adem.202100624
摘要
Herein, the effect of the addition of Ni‐coated carbon nanotubes (CNTs) on the microstructure, mechanical properties, and morphology of zirconia porous cellular structures is studied, aiming to increase their mechanical strength. Highly porous structures of monolithic zirconia (ZrO 2 ) and zirconia reinforced with Ni‐doped CNTs (ZrO 2 + CNT/Ni) are fabricated through the replica method. Scanning electron microscopy and micro‐computed tomography (microCT) analyses show that ZrO2 + CNT/Ni specimens present lower overall porosity (88.0%) than monolithic ZrO 2 (93.8%), indicating improved sintering kinetics. Compressive tests for the ZrO 2 + CNT/Ni samples result in a compressive strength of 0.82 ± 0.10 MPa, a threefold value of that of the monolithic sample (0.25 ± 0.07 MPa). The ZrO 2 + CNT/Ni samples also present a higher elastic modulus (41.02 ± 4.94 MPa) than the ZrO 2 ones (21.92 ± 5.40 MPa). Thus, the addition of Ni‐coated CNTs significantly improves the strength of highly porous zirconia cellular structures.
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