Experimental studies have been conducted on temperature separation and LOX separation both for straight and conical vortex tubes with six convergent nozzles for different dc/D and L/D ratios. Straight vortex tubes are found to perform better for temperature separation though they are not suitable for LOX separation as compared to conical vortex tubes. LOX purity of about 96% with a separation efficiency of about 14% has been achieved with conical vortex tube with L/D of 10. High LOX purity and separation efficiency obtained through experiments on staging of vortex tubes are discussed.