化学
银纳米粒子
多糖
纳米颗粒
傅里叶变换红外光谱
核化学
透射电子显微镜
粒径
有机化学
化学工程
纳米技术
材料科学
工程类
物理化学
作者
Yongshuai Jing,Jiaying Li,Yuwei Zhang,Ruijuan Zhang,Yuguang Zheng,Beibei Hu,Liqing Wu,Danshen Zhang
标识
DOI:10.1016/j.ijbiomac.2021.04.178
摘要
A novel polysaccharide (GLP) with a molecular weight of 1.37 × 105 Da was purified from the roots of G. littoralis. Using monosaccharide composition, methylation analysis, GC–MS, 1D and 2D NMR, the structure of GLP was determined to be a 1 → 4)-α-D-Glcp glycoside linkage, while the terminal group of 1→)-α-D-Glcp was bonded to the main chain via O-6. Then, GLP-NPs were prepared by nano-precipitation method, the particle size of GLP-NPs was 288.4 nm and PDI was 0.340. GLP-NPs-AgNPs were prepared using GLP-NPs as reducing agent. GLP-NPs-AgNPs were characterized by ultraviolet-visible spectrophotometer (UV–Vis), Fourier transform infrared spectroscopy (FT-IR), transmission electron microscope (TEM) and X-ray diffraction (XRD). The yield of GLP-NPs-AgNPs was 38.77%, the particle size was 12.5 nm and the chelation rate of silver nanoparticles with polysaccharides was 67.5%. GLP-NPs-AgNPs had better antioxidant and antibacterial activities than GLP and GLP-NPs. In the present work, a simple and eco-friendly approach for the synthesis of silver nanoparticles (AgNPs) using G. littoralis polysaccharides nanoparticles (GLP-NPs) as reducing agent.
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