Synthesis Study of Lu<SUB>3</SUB>Al<SUB>5</SUB>O<SUB>12</SUB>(Ce) Nanoscaled Powder by Co-precipitation
材料科学
核化学
放射化学
结晶学
化学
作者
Jian-Jun XIE,Ying Shi,Yao-Ming HU,Qi-Wei CHEN,Jian-Lin SHI
出处
期刊:Journal of Inorganic Materials [Science Press] 日期:2009-02-16卷期号:24 (1): 79-82被引量:7
标识
DOI:10.3724/sp.j.1077.2009.00079
摘要
Ce3+-doped Lutetium aluminum garnet Lu3Al5O12 phosphors were prepared by an anti co-precipitation from mixing solution of lutetium,aluminum and cerium nitrates using the ammonium hydrogen carbonate as precipitate,followed by the calcination at low temperatures.TG-DTA,FTIR,XRD,TEM and Photoluminescence were used to characterize the as-prepared phosphors.The calcining temperature has distinctly influence on the particle size and the photoluminescence of the prepared Lu3Al5O12(Ce) powders.The resulted Lu3Al5O12(Ce) powder calcined at 1000℃ for 2h has an average particle size of 30nm.And its photoluminescence is the strongest among the powders calcined in the range from 850℃ to 1200℃.