材料科学
微观结构
放电等离子烧结
纳米复合材料
碳化物
粒度
碳纳米管
晶粒生长
复合材料
合金
硬质合金
冶金
作者
Hao Jiang,Zhiwei Zhao,Yanju Qian,Yaohua Yan,Yongquan Lei,Zhao Hui Zhang,Shijie Zhang,Zheng Chen,Shun Wang,Xiaohan Lu
标识
DOI:10.1016/j.jmrt.2023.08.118
摘要
Obtaining cemented carbides with smaller WC grain size and better properties is key to their wider application. Ultrafine cemented carbides were prepared by using spark plasma sintering (SPS) with nano VC-Cr3C2 as nanocomposite grain growth inhibitors (NGGIs) and multi-walled carbon nanotubes (MWCNTs) as reinforcing materials. The effects of NGGIs and MWCNTs on the microstructure and mechanical properties of alloys were evaluated. The results indicated that the specimens (0.5 wt % NGGIs and 0.4 wt % MWCNTs) prepared at 1350 °C for 8 min under a pressure of 50 MPa have enhanced mechanical properties (HV 2520.85 kgf/mm2, KIC 13.26 MPa·m1/2) and a homogeneous microstructure. The grain size of WC is suppressed (the average grain size is 200-400 nm). NGGIs can prevent the dissolution of W and C in liquid Co, thereby inhibiting the growth of WC grains. The uniform dispersion of MWCNTs in WC matrix mobilizes their fiber-reinforcement effect. The combination of NGGIs, MWCNTs, and SPS can improve the mechanical properties and optimize the microstructure of the alloy.
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