材料科学
热重分析
差示扫描量热法
傅里叶变换红外光谱
涂层
核化学
羧甲基纤维素
化学工程
动态光散射
高分子化学
复合材料
化学
纳米颗粒
钠
工程类
物理
冶金
热力学
纳米技术
作者
El Hassan Boutriouia,Taha El Assimi,Mustapha Raihane,Rédouane Beniazza,Hicham Ben Youcef,Mehdi Khouloud,Mohamed Hassen V. Baouab,Abdelkrim El Kadib,Mohammed Lahcini
标识
DOI:10.1016/j.porgcoat.2022.107102
摘要
In the perspective of preparing coating material of water-soluble fertilizer with controlled and slow-release property, polymethyl methacrylate (PMMA) was grafted from carboxymethyl cellulose (CMC) through in-situ polymerization using potassium persulfate (KPS) as initiator. The prepared copolymers (PMMA-g-CMC) were fully characterized using Transform Infrared Spectroscopy (FTIR), Thermogravimetric analysis (TGA), Differential Scanning Calorimetry (DSC), Dynamic light scattering (DLS), X-Ray diffraction (XRD), Brunauer Emmett Teller (BET), Scanning electron microscopy (SEM) and mechanical tensile testing. The molecular weight (Mn) was also evaluated using the size exclusion chromatography (SEC). Next, conventional water-soluble diammonium phosphate (DAP) fertilizer was coated by the prepared copolymers using laboratory rotary drum. The coating effectiveness was evaluated in terms of its uniformity and thickness. The successfully coated nanomaterials significantly delay the release rate of nitrogen (N) and phosphorus (P) in water and soil, compared to their release using uncoated fertilizers. Finally, aerobic biodegradation of the coating agent was also demonstrated.
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