染色
超临界二氧化碳
活性染料
材料科学
分散染料
基础(拓扑)
化学工程
扫描电子显微镜
二氧化碳
高分子化学
复合材料
化学
超临界流体
有机化学
数学分析
工程类
数学
作者
Dalia Zaghloul,Tarek Abou Elmaaty,Keigo Nakamura,Isao Tabata,Teruo Hori,Kazumasa Hirogaki
标识
DOI:10.1016/j.supflu.2021.105243
摘要
This paper demonstrates the impact of an organic base on dyeing of cotton fabric using a fluorotriazine-based reactive disperse dye under waterless dyeing conditions with supercritical carbon dioxide (scCO2). The cotton fabric was dyed without pre-treatment. The system parameters, including temperature, pressure, time, and dye concentration, were examined. The systematic variation in the parameters indicated that the optimal coloration was achieved by adding 300 mM of α-picoline as an alkali at 120 °C and 25 MPa under scCO2. The dye structure was determined using infrared and nuclear magnetic resonance spectral data, showed a good agreement with the structure proposed. The morphological structure was partially identical with no damage to the cotton, as determined using scanning electron microscopy. The results indicated that fluorotriazine-based dye has a high coloring behavior, with the color strength, leveling properties, and staining fastness rated at 4–5 in terms of a dyeing medium with α-picoline.
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