双功能
纳米复合材料
抗菌剂
催化作用
X射线光电子能谱
生物相容性
傅里叶变换红外光谱
材料科学
甲基橙
核化学
超顺磁性
化学工程
磁化
化学
纳米技术
有机化学
光催化
冶金
工程类
物理
量子力学
磁场
作者
Juan Shi,Jie Zheng,Ben Liang,Fuqiang Song,Jin Wang,Sheng Guo,Hongguang Ge,Yanhong Gao,Tianlei Zhang
标识
DOI:10.1016/j.colsurfa.2023.131402
摘要
Integrating metal nanocomposites into a matrix is a promising approach for improving the material chemical and physical properties. Herein, Fe3O4 @SiO2 @mTiO2-NH2 @Ag (FSTN-Ag) nanocomposites were synthesized by reducing silver nitrate onto amino-modified double core-shell Fe3O4 @SiO2 @mTiO2-NH2 (FSTN) nanospheres. TEM, XRD, XPS, BET, TOC, UV–vis and FTIR spectrum were used to characterize the nanocomposites. The magnetic FSTN-Ag nanocomposites possessed a core–shell structure, with a specific surface area of 113.6 m2/g, pore volume of 0.122 cm3/g, magnetization saturation of 46.17 emu/g, and Ag mean diameter of 2.8 nm. The FSTN-Ag demonstrated high catalytic activity on reducing methyl orange (MO) and its catalytic ability could kept 85% after 5 cycles. The FSTN-Ag also effectively inhibited S. aureus and E. coli in 20 min by up to 99% or 100%, respectively. It was speculated that the antimicrobial mechanism involved the interaction of Ag+ derived from FSTN-Ag with functional groups of vital enzymes and proteins as well as strong oxidation of reactive oxygen species resulting in bacterial death. In view of the magnetic separation, biocompatibility and recyclability, the FSTN-Ag is expected to become a potential multifunctional material for biomedical and environmental remediation.
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