收缩率
材料科学
陶瓷
烧结
3D打印
非线性系统
选择性激光烧结
复合材料
正规化(语言学)
强度(物理)
图层(电子)
优化设计
过程(计算)
机械工程
均方误差
实验设计
计算机科学
响应面法
过程控制
作者
Xiaohui Jiang,Jirui Liu,Yan Wang,Zhijun Ding,Jie Liu,Li Ji,Peng Li
标识
DOI:10.1016/j.matdes.2025.115053
摘要
• Precise control of sintering shrinkage in micro-nano ceramic 3D printing for high-accuracy applications. • Development of a shrinkage prediction model using orthogonal design with supplementary points and regularization regression. • The model reveals nonlinear effects of layer thickness, exposure time, and light intensity on shrinkage. • Validated through TPMS structures, demonstrating practical potential in ceramic additive manufacturing. Micro-nano ceramic 3D printing technology offers unique advantages in the fields of microfluidic chips and biological scaffolds through layer-by-layer additive manufacturing. However, its sub-micron accuracy requirements make the control of sintering shrinkage particularly critical. In this study, the sintering shrinkage of micro-nano ceramic 3D printing was investigated as the primary research focus. An orthogonal experimental design combined with supplementary experimental points was used to construct a shrinkage prediction model, incorporating the nonlinear response of materials. By introducing higher-order interaction terms and applying regularization regression (LASSO), the model’s fitting accuracy and generalization ability were improved. The experimental results indicate that the prediction model yields a low mean squared error (MSE = 0.2507) and effectively captures the nonlinear effects of printing layer thickness, exposure time, and light source intensity on sintering shrinkage. Furthermore, optimal process control parameters were identified, with a combination of h = 0.01 mm and I = 25200 μW/cm 2 ensuring moderate shrinkage (23–24 %). Finally, the model’s reliability and accuracy were validated in practical applications, using it to guide the preparation of ceramic TPMS structures. This study provides new theoretical support and technical pathways for micro-nano scale process control in ceramic additive manufacturing
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