The vaporous and particulate organic pollutants were simultaneously sampled by GDX 101 and glass fiber filters (GF) respectively After organic pollutants in GDX 101 and the filters were separately extracted,they were analyzed qualitatively with GC MS.It's observed that the kinds and content of the particulate organic pollutants were higher than them of the vaporous one.Organic pollution in the air of industry area was serious than in the air of living area.And pollution of burning coal and burning oil was main.