萃取(化学)
槲皮素
化学
产量(工程)
色谱法
沸腾
溶剂
水萃取
沸点
甲醇
热水抽汽
材料科学
有机化学
抗氧化剂
冶金
作者
Min Jung Ko,Chan Ick Cheigh,Sang Woo Cho,Myong Soo Chung
标识
DOI:10.1016/j.jfoodeng.2010.09.008
摘要
Subcritical water could be an excellent alternative to organic solvent as a medium for extracting flavonol quercetin, due to its temperature-dependent selectivity, safety, efficiency of recovery, and lower cost. This study investigated the application of subcritical water extraction (SWE) of quercetin from onion skin and evaluated the effect of key operation conditions by varying the temperature (100–190 °C), extraction time (5–30 min), and mixture ratio of onion skin and diatomaceous earth (DE) (0.5:3.5–2:2) under high pressure (90–131 bar). The maximum yield of quercetin (16.29 ± 0.75 mg/g onion skin) was obtained at extraction temperature of 165 °C, extraction time of 15 min, mixture ratio of 1.5:2.5 for onion skin and DE. The SWE was compared with three conventional extraction methods in terms of the efficiency. The quercetin yield by SWE was over eight-, six-, and fourfold greater than those obtained using the ethanol, methanol, and water-at-boiling-point extraction methods, respectively.
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