石墨烯
材料科学
纳米复合材料
水溶液中的金属离子
氧化物
扫描电子显微镜
纳米技术
吸附
离子
电化学
化学工程
金属
电化学气体传感器
纳米颗粒
电极
复合材料
冶金
有机化学
化学
工程类
物理化学
标识
DOI:10.1166/sam.2020.3607
摘要
The purpose of this study was to explore the application of graphene-based nanocomposites in electrochemical detection of heavy metal ions. In this study, Graphene oxide (GO) was synthesized with improved Hummers method, and flower-like MoS 2 /rGO nanocomposite was synthesized with hydrothermal method and used as electrode modification material. In addition, scanning electron microscopy (SEM) and X-ray images were used to observe the characterization of the prepared samples and to detect the sensitivity of four heavy metal ions under optimal experimental conditions. The results showed that the reduced graphene oxides were coated with a large number of flower-like MoS 2 and laid on the reduced graphene oxides. And in electrochemical experiments, adsorption experiments and interference tests, MoS 2 /rGO nanocomposites showed satisfactory performance for Pb(II). Therefore, this study provided a new strategy for the development of new nanocomposites composites as electrochemical sensors to detect the heavy metal ions in the aquatic environment.
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