Enhanced Photo-Assisted Acetone Gas Sensor and Efficient Photocatalytic Degradation Using Fe-Doped Hexagonal and Monoclinic WO3 Phase−Junction

材料科学 光电流 光催化 罗丹明B 单斜晶系 相(物质) 兴奋剂 分析化学(期刊) 六角相 相对湿度 吸附 催化作用 光化学 光电子学 化学 有机化学 晶体结构 物理 热力学
作者
Jichao Wang,Weina Shi,Xue-Qin Sun,Fang-Yan Wu,Yu Li,Yuxia Hou
出处
期刊:Nanomaterials [Multidisciplinary Digital Publishing Institute]
卷期号:10 (2): 398-398 被引量:24
标识
DOI:10.3390/nano10020398
摘要

The development of WO3-based gas sensors for analysis of acetone in exhaled breath is significant for noninvasive diagnosis of diabetes. A series of Fe-doped hexagonal and monoclinic WO3 phase−junction (Fe−h/m−WO3) sensors were synthesized by the hydrothermal calcination method, and the influences of operating temperature and light irradiation on the response were studied. Under light emitting diode (LED) illumination, Fe−h/m−WO3 exhibited higher responses to acetone than those of the undoped WO3-based sensors at an operating temperature of 260 °C with 90% relative humidity, and good linearity between response and acetone concentration (0.5 to 2.5 ppm) was achieved under the 90% relative humidity condition. Meanwhile, the optimal Fe−h/m−WO3 sensor exhibited high selectivity and stability for a duration of three months. The excellent sensing performance of Fe−h/m−WO3 was attributed to the formation of phase−junction and Fe doping, and these were beneficial for the separation of photon−generated carriers and oxygen adsorption on the WO3 surface, promoting the generation of superoxide radicals, which was demonstrated by electron paramagnetic resonance and photocurrent tests. Additionally, the Fe−doped WO3 phase−junction sample also showed good photocatalytic performance for rhodamine B degradation. This study may provide some insights into rational design of new types of gas sensors and offer an alternative for noninvasive diagnosis of diabetes.
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