检出限
石墨烯
异烟肼
材料科学
线性范围
选择性
电化学气体传感器
再现性
纳米复合材料
氧化物
碳糊电极
电极
纳米技术
电化学
色谱法
化学
循环伏安法
有机化学
肺结核
冶金
催化作用
物理化学
病理
医学
作者
Zahra Zareie,Navid Nasirizadeh,Mohammad Mirjalili,Masoud Rohani-Moghadam,Mohammadali Shirgholami
出处
期刊:Measurement
[Elsevier]
日期:2022-02-01
卷期号:189: 110431-110431
被引量:5
标识
DOI:10.1016/j.measurement.2021.110431
摘要
In this research, an effective, selective and accurate method for determining the isoniazid (INH) residues is presented based on screen printed carbon electrode (SPCE) modified with graphene oxide/gold nanourchin/layer molecular imprinted polymer. The morphological properties of the suggested sensor were explored by FESEM, FTIR, EDX techniques as well as its electrochemical characteristics versus isoniazid were invigilated in detail. The proposed sensor was capable of measuring the isoniazid in the linear range of 2.5–850.0 nM with a detection limit of 0.85 nM. One of the excellent features of this sensor is its good selectivity to INH in the presence of anionic species from these families of drugs. This sensor has an acceptable price, speed, detection limit, selectivity, reproducibility and fast response time compared to other isoniazid quantification sensors. The proposed sensor was used to measure the INH values in biological samples such as blood and urine with appropriate recovery percentage.
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