Microstructural origin and control mechanism of the mixed grain structure in Ni-based superalloys

动态再结晶 等轴晶 索尔夫斯 材料科学 再结晶(地质) 微观结构 粒度 晶界 高温合金 应变率 变形机理 冶金 电子背散射衍射 热加工 地质学 古生物学
作者
Baoyun Zhang,Zhaotian Wang,Hao Yu,Yongquan Ning
出处
期刊:Journal of Alloys and Compounds [Elsevier BV]
卷期号:900: 163515-163515 被引量:86
标识
DOI:10.1016/j.jallcom.2021.163515
摘要

• As an incomplete recrystallization, mixed grain structure with numerous dislocation tangle in Non-DRX region. • Homogeneous equiaxed grains can be obtained at the optimum processing parameters identified by 3D processing map. • Grain growth may be responsible for the near< 001 > compression texture detected in super-solvus deformation. • DDRX and CDRX occur simultaneously in microstructure control for mixed grain structure. • DDRX is the dominant nucleation mechanism while CDRX belongs to the assistant one. Mixed grain structure, as an incomplete recrystallization, should be homogenized and refined by subsequent processing to improve the mechanical properties of the aeroengine components. The microstructural origin and control mechanism is quite necessary for the microstructure homogenizing and grain refining through thermo-mechanical processing. In present research, microstructural origin and control mechanism of the mixed grain structure have been conducted deeply. With the consideration of temperature drop in practical industrial forging, the optimum processing parameters can be determined as 1110–1140 °C/1.0 s −1 to obtain homogeneous equiaxed grains. The microstructure evolution corresponding to the identified optimal parameters, viz., deformation temperature and strain rate, were systematically investigated. Higher dynamic recrystallization (DRX) fraction and coarser DRX grains can be observed at super-solvus temperature deformation (1140 °C). In addition, sub-solvus deformation (1110 °C) shows random orientated distribution while near< 001 > compression texture can be detected in super-solvus deformation. Particular attention was paid to the DRX mechanisms during hot deformation. Discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) occur simultaneously, and the synergistic effect of them contributes to microstructure control. Moreover, DDRX characterized by grain boundary bulging dominants the microstructure control. Progressive subgrain rotation labeled as CDRX can be regarded as an important assistant mechanism. The findings would provide theoretical support for microstructure control of Ni-based superalloys with mixed grain structure, which is of vital importance for components to obtain excellent performance.
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