同步加速器                        
                
                                
                        
                            金属间化合物                        
                
                                
                        
                            合金                        
                
                                
                        
                            磁场                        
                
                                
                        
                            材料科学                        
                
                                
                        
                            定向凝固                        
                
                                
                        
                            相(物质)                        
                
                                
                        
                            旋转磁场                        
                
                                
                        
                            微观结构                        
                
                                
                        
                            冶金                        
                
                                
                        
                            磁铁                        
                
                                
                        
                            凝聚态物理                        
                
                                
                        
                            光学                        
                
                                
                        
                            化学                        
                
                                
                        
                            物理                        
                
                                
                        
                            量子力学                        
                
                                
                        
                            有机化学                        
                
                        
                    
            作者
            
                Zihan Song,Élodie Boller,Alexander Rack,Peter Lee,Biao Cai            
         
                    
        
    
            
            标识
            
                                    DOI:10.1016/j.jallcom.2022.168691
                                    
                                
                                 
         
        
                
            摘要
            
            Magnetic fields have been widely used to control solidification processes. Here, high-speed synchrotron X-ray tomography was used to study the effect of magnetic fields on solidification. We investigated vertically upward directional solidification of an Al-Si-Cu based W319 alloy without and with a transverse magnetic field of 0.5 T while the sample was rotating. The results revealed the strong effect of a magnetic field on both the primary α-Al phase and secondary β-Al5FeSi intermetallic compounds (IMCs). Without the magnetic field, coarse primary α-Al dendrites were observed with a large macro-segregation zone. When a magnetic field is imposed, much finer dendrites with smaller primary arm spacing were obtained, while macro-segregation was almost eliminated. Segregated solutes were pushed out of the fine dendrites and piled up slightly above the solid/liquid interface, leading to a gradient distribution of the secondary β-IMCs. This work demonstrates that rotating the sample under a transversal magnetic field is a simple yet effective method to homogenise the temperature and composition distributions, which can be used to control the primary phase and the distribution of iron-rich intermetallics during solidification.
         
            
 
                 
                
                    
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