选区衍射
材料科学
粒径
纳米颗粒
透射电子显微镜
比表面积
粒度分布
衍射
打赌理论
粒子(生态学)
惰性气体
电弧
Crystal(编程语言)
铜
电子衍射
化学工程
阳极
分析化学(期刊)
纳米技术
冶金
复合材料
化学
光学
电极
物理化学
色谱法
有机化学
吸附
海洋学
催化作用
计算机科学
程序设计语言
工程类
地质学
物理
作者
Hong Xia Qiao,Zhi Qiang Wei,Ming Zhou,Zhong Mao He
出处
期刊:Advanced Materials Research
日期:2010-01-01
卷期号:92: 163-169
标识
DOI:10.4028/www.scientific.net/amr.92.163
摘要
Copper nanoparticles were successfully prepared in large scales by means of anodic arc discharging plasma method in inert atmosphere. The particle size, specific surface area, crystal structure and morphology of the samples were characterized by X-ray diffraction (XRD), BET equation, transmission electron microscopy (TEM) and the corresponding selected area electron diffraction (SAED). The experiment results indicate that the crystal structure of the samples is fcc structure as same as that of the bulk materials. The specific surface area is is 11 m2/g, with the particle size distribution ranging from 30 to 90 nm, the average particle size about 67nm obtained from TEM and confirmed from XRD and BET results. The nanoparticles have uniform size, higher purity, narrow size distribution and spherical shape can be prepared by this convenient and effective method.
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