三聚氰酸
三聚氰胺
热稳定性
材料科学
熔点
Crystal(编程语言)
水溶液
分析化学(期刊)
粉末衍射
核化学
蒸发
热分析
活化能
化学工程
结晶学
热的
化学
物理化学
有机化学
复合材料
气象学
工程类
程序设计语言
计算机科学
物理
热力学
作者
V. Sangeetha,N. Kanagathara,R. Radhakrishnan Sumathi,N. Sivakumar,G. Anbalagan
出处
期刊:Journal of materials
[Hindawi Limited]
日期:2013-03-06
卷期号:2013: 1-7
被引量:16
摘要
Melamine cyanurate, an organic crystalline complex was, synthesized by evaporation of an aqueous solution containing equimolar quantities of melamine and cyanuric acid. The synthesized compound has been subjected to various characterizations like Powder XRD, FT-IR, TG-DTG, SEM, and SHG. The presence of sharp diffraction peaks in the XRD confirms that the products are highly crystalline. The average particle size was calculated using the Debye-Scherrer formula, and it was found to be 3.067 μ m. Thermal behavior of the grown crystal has been studied by TG-DTG analysis. From TG-DTG, it is found that the title crystal possesses good thermal stability. The activation energy was calculated using the Broido, Coats-Redfern, and Horowitz-Metzger methods. A sharp peak exothermic peak at 405.40°C was assigned as the melting point of the title material. SEM reveals the morphology of the synthesized salt. No detectable signal was observed during the Kurtz-Perry technique.
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