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 To enable co-assembly with fucoidan, γ-PGA was functionalized via EDC/NHS-mediated amidation [31] with 3-aminophenylboronic acid (3-APBA), yielding γ-PGAB. 1H NMR results showed that the peaks at δ = 1.89 and 4.16 ppm correspond to the methylene and methine groups of γ-PGA, while δ = 2.35 ppm represents the γ-position proton (Figure 1a) [24, 32]. After modification, new aromatic peaks appeared at δ = 7.43, 7.54, and 7.72 ppm, consistent with the benzene ring of 3-APBA [33], confirming the succe |
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