化学
酞菁
热重分析
金属
磁化率
锌
镍
铜
钴
分子间力
热稳定性
碎片(计算)
质谱
磁矩
结晶学
无机化学
质谱法
分子
有机化学
计算机科学
物理
凝聚态物理
操作系统
色谱法
作者
B. N. Narahari Achar,G. M. Fohlen,Joseph Parker,J. Keshavayya
出处
期刊:Polyhedron
[Elsevier]
日期:1987-01-01
卷期号:6 (6): 1463-1467
被引量:193
标识
DOI:10.1016/s0277-5387(00)80910-9
摘要
Preparation of pure metal(II) 4,9,16,23-phthalocyanine tetraamine 2-hydrates of copper, cobalt, nickel and zinc are reported. Elemental analysis, electronic spectra, FT-IR spectra, powder X-ray diffraction, magnetic-susceptibility measurements, dynamic thermogravimetric MS and GC-MS spectral studies are carried out to check the purity, structural integrity, thermal stability and mode of fragmentation of these complexes. Magnetic-susceptibility measurements showed a variation in the magnetic moments of these complexes with magnetic field strength, indicating the presence of a co-operative intermolecular effect.
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