热液循环
扫描电子显微镜
纳米颗粒
拉曼光谱
透射电子显微镜
材料科学
粒径
化学工程
肺表面活性物质
磁性纳米粒子
分析化学(期刊)
水热合成
杂质
粒子(生态学)
纳米技术
化学
复合材料
光学
色谱法
有机化学
工程类
地质学
物理
海洋学
作者
Manish Srivastava,Animesh K. Ojha,S. Chaubey,Jay Singh,Prashant K. Sharma,Avinash C. Pandey
标识
DOI:10.1016/j.jallcom.2010.03.245
摘要
Impurity free α-Fe2O3 nanoparticles have been synthesized by hydrothermal method using two different precursors, FeCl3·6H2O and Fe(NO3)3·9H2O. The physical properties of the synthesized nanoparticles were investigated by X-ray diffraction (XRD), Raman spectroscopy (RS), scanning electron microscope (SEM) high resolution transmission electron microscope (HR-TEM) and vibrating sample magnetometer (VSM). The average particle size of the nanoparticles synthesized using FeCl3·6H2O and Fe(NO3)3·9H2O was calculated to be ∼60 and ∼87 nm, respectively. The magnetic properties of the α-Fe2O3 nanoparticles synthesized using both the precursors were found be quite different, which may be attributed to the different particle size of the nanoparticles.
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