微波消解
原子吸收光谱法
石墨炉原子吸收
化学
金属
分析化学(期刊)
质谱法
重金属
消化(炼金术)
检出限
色谱法
环境化学
量子力学
物理
有机化学
出处
期刊:Chinese Journal of Spectroscopy Laboratory
日期:2011-01-01
摘要
The sample of Chinese traditional mechine gamboge was digested with microwave digestion system,Mn,Cu,Fe were determined by flame atomic absorption spectometry,and Cr,Cd,Pb were determined by graphite furnace atomic absorption spectrometry.The recovery of six heavy metal was in the range of 92.0%—102.0%,RSD was 0.99%—2.49%.Amounts of the six heavy metal found in the Chinese traditional mechine gamboge were as follows: Mn 65.7μg/g,Cu 2.37μg/g,Fe 48.5μg/g,Cd 0.012μg/g,Pb 5.10μg/g,the metal of Cr was not found.The method is easy and accurate and can be used in the determination of heavy metals in traditional Chinese medicine.
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