材料科学
设计-专家
硅酸钾
钛
极限抗拉强度
中心组合设计
硅酸钠
电极
氧化物
冶金
复合材料
金红石
响应面法
化学工程
化学
色谱法
物理化学
工程类
作者
Nwigbo Solomon Chuka,Okpe Adanma Uzoma,Echezona Nnaemeka Obika,Chinweze Arinze Everest,Igwebuike Godknows Chibueze
标识
DOI:10.1177/16878132221108265
摘要
A stainless steel flux for manual metal arc welding (MMAW) has been developed. The coated electrode is a rutile electrode whose basic components are titanium (IV) oxide and stainless steel powder. Some of the other components were substituted; the more popular but expensive potassium silicate binder was replaced with readily available sodium silicate binder. For the binder to perform effectively, it was enriched with potassium carbonate, which was sourced locally from palm bunch. Cellulose, a good gas former was replaced with starch, which was gotten from cassava. The components were sieved into 75 µm particle size. The experimental design was set up using Central Composite Design in Design Expert software. The design varied the percentage composition of calcium carbonate, binder, titanium (IV) oxide, silicon (IV) oxide, and stainless steel powder. Twenty-six (26) test samples were produced using the central composite design tool of the design expert software and tested for tensile strength. The experimental results were analyzed and optimized using Response Surface Methodology and Validated using the ANOVA tool of the Design Expert software. An optimal composition of 10% CaCO 3 , 13% Binder, 13% Titanium oxide, 12% silicon (IV) oxide, and 36% stainless steel powder were obtained to give a corresponding 539.7 N/mm 2 tensile strength.
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