纳米压痕
材料科学
聚乙烯醇
扫描电子显微镜
复合材料
纳米复合材料
石墨烯
X射线光电子能谱
色散(光学)
透射电子显微镜
弹性模量
化学工程
纳米技术
光学
物理
工程类
作者
Andres Felipe Pava,Mateo Duarte García,Sara N. Herrera,J. M. Meza,Jose Martin Herrera Ramírez,César Augusto Isaza Merino
出处
期刊:Journal of Engineering Materials and Technology-transactions of The Asme
[American Society of Mechanical Engineers]
日期:2023-08-18
卷期号:146 (1)
摘要
Abstract Polyvinyl alcohol (PVA) was investigated as a vehicle for incorporating thermally reduced graphene oxides (TRGOs) into metal matrix composites (MMCs). The TRGOs were synthesized using the modified Hummers’ method and characterized using scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). The PVA/TRGOs nanocomposites were synthesized using the solution mixing technique. The dispersion qualification and quantification of TRGOs in PVA were evaluated through tension and nanoindentation tests, as well as elastic modulus mapping by nanoindentation. The results demonstrated a good dispersion of TRGOs in the PVA matrix, resulting in exceptional mechanical properties. The dispersion time and energy variables were carefully controlled, leading to a good dispersion degree verified by the quantification analysis. Furthermore, preliminary studies confirmed the effectiveness of the PVA as an inclusion vehicle for nanoreinforcements in metallic matrices.
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