异甘草素
葡聚糖
硅胶
蝙蝠葛甾醇
化学
部
毛竹
香兰素
色谱法
柱色谱法
高效液相色谱法
碳-13核磁共振
核化学
有机化学
立体化学
植物
生物
酶
竹子
作者
Bin Li,Yong Zhang,Wenpeng Du,Hongdong Liu,Bo Liu,Xue-wen Lai,Peng Xu
出处
期刊:PubMed
[National Institutes of Health]
日期:2015-12-01
卷期号:38 (12): 2535-7
被引量:3
摘要
To investigate the chemical constituents from the shoot of Phyllostachys edulis.Normal-phase, reversed-phase silica gel, Sephadex LH-20 porous polymer gel column and HPLC chromatography were used for isolation. Spectroscopic methods (13C-NMR, 1H-NMR, DEPT and EI-MS) were used for identification.Eleven compounds were isolated and elucidated, which were skimmin(I), liquiritienin(II),1-(4-hydroxy-3-methoxyphenyl)-1-propanone(III), syringicaldehyde(IV), vanillin(V), isoliquiritigenin(VI), 4-hydroxybenzoic acid(VII), methyl p-hydroxy benzeneacetate (VIII), 5,7-dihydroxy-8-methoxyflavone (IX), daucosterol(X) and β-sitosterol(X).All the compounds are obtained from this plant for the first time, and compounds VI, VIII and IX are firstly isolated from the plants of this genus.
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