材料科学
立方氧化锆
陶瓷
扫描电子显微镜
表面粗糙度
多孔性
化学工程
蚀刻(微加工)
吸附
惰性
表面光洁度
复合材料
表面改性
千分尺
图层(电子)
化学
有机化学
物理
光学
工程类
作者
Damian S. Nakonieczny,Aleš Slíva,Z. Paszenda,Marianna Hundáková,Gabriela Kratošová,Sylva Holešová,Justyna Majewska,Piotr Kałużyński,Sajjan Kumar Sathish,Gražyna Simha Martynková
出处
期刊:Crystals
[MDPI AG]
日期:2021-10-12
卷期号:11 (10): 1232-1232
被引量:15
标识
DOI:10.3390/cryst11101232
摘要
In order for bioceramics to be further used in composites and their applications, it is important to change the surface so that the inert material is ready to interact with another material. Medical grade alumina and zirconia ceramic powders have been chemically etched with three selected acidic mixtures. Powder samples were taken for characterization, which was the key to evaluating a successful surface change. Changes in morphology, together with chemical composition, were studied using scanning electron microscopy, phase composition using X-ray diffraction methods, and nitrogen adsorption/desorption isotherms are used to evaluate specific surface area and porosity. The application of HF negatively affected the morphology of the material and caused agglomeration. The most effective modification of ceramic powders was the application of a piranha solution to obtain a new surface and a satisfactory degree of agglomeration. The prepared micro-roughness of the etched ceramic would provide an improved surface of the material either for its next step of incorporation into the selected matrix or to directly aid in the attachment and proliferation of osteoblast cells.
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