Twisting Chiral Aggregation‐Induced Emission Macrocycles into a Microhelix with Boosted Circularly Polarized Luminescence

values and helical structure formation. This work not only advances the design of chiral macrocycles but also provides new insights into the relationship between molecular structure and supramolecular assembly, paving the way for the development of advanced chiral materials with potential applications in optics, sensing, and nanotechnology.