高分辨率透射电子显微镜
X射线光电子能谱
材料科学
扫描电子显微镜
透射电子显微镜
退火(玻璃)
复合数
纳米颗粒
微观结构
肖特基势垒
化学工程
分析化学(期刊)
衍射
纳米技术
核化学
复合材料
化学
色谱法
光学
光电子学
物理
工程类
二极管
作者
Chao Zhang,Yunchun Huan,Ying Li,Yifan Luo,Marc Debliquy
标识
DOI:10.1007/s40145-021-0530-x
摘要
Abstract In order to detect low concentrations of volatile organic compounds (VOCs) for the early diagnosis of lung cancer, sensors based on hollow spheres of In 2 O 3 were prepared through the soft template method. Ag nanoparticle decorated In 2 O 3 composites were synthesized via dipping and annealing. The microstructure, phase composition, element distribution, and state of Ag were analyzed by the scanning electron microscopy (SEM), X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), and X-ray photoelectron spectroscopy (XPS). The gas sensing tests showed that Ag-In 2 O 3 sensors had the highest response to isopropanol at 300 °C. The best response of Ag-In 2 O 3 composite sensor was 5.2, which had a significant improvement compared with only In 2 O 3 . Moreover, the response and recovery time of Ag-In 2 O 3 composite sensor was significantly shortened. The improved sensing properties of Ag-In 2 O 3 composite sensor could be attributed to the Schottky barrier created at Ag-In 2 O 3 interface and catalytical effect of Ag.
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