锌
微晶
草酸
材料科学
草酸盐
纳米颗粒
傅里叶变换红外光谱
螯合作用
氧化物
化学工程
无机化学
核化学
纳米技术
化学
冶金
工程类
作者
Gráinne M. Duffy,Suresh C. Pillai,Declan E. McCormack
标识
DOI:10.1088/0964-1726/16/4/052
摘要
Zinc oxide nanoparticles have been processed from a novel isophthalate precursor. In contrast to those processed from an oxalate precursor, this material exhibits three-dimensional, non-directional aggregation behaviour. Such non-directional aggregation of uniaxial crystallites may allow for the production of structures with a higher proportion of catalytically active surfaces than can be prepared through conventional sol–gel methods. XRD, FTIR, TEM and SEM were used to characterize the synthesized materials. Zinc oxide particles synthesized by using isophthalic acid (C 6 H 4 -1,3-(COOH) 2 ) are found to be slightly smaller than the previously reported materials prepared through chelation with oxalic acid (H 2 C 2 O 2 ·2H 2 O).
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