纳米团簇
高分辨率透射电子显微镜
石墨烯
材料科学
氧化锡
检出限
电化学气体传感器
电化学
氧化物
过氧化氢
透射电子显微镜
扫描电子显微镜
化学工程
纳米技术
化学
电极
复合材料
冶金
有机化学
色谱法
物理化学
工程类
作者
Chun-Mei Zhang,Lei Li,Jian Ju,Wei Chen
标识
DOI:10.1016/j.electacta.2016.05.151
摘要
Hydrogen peroxide (H2O2) is closely related to people’s life in a lot of respects, including food, health, and environment and so on. High performance detection of H2O2 is of importance in chemical and biological fields. In this study, we synthesized reduced graphene oxide-supported tin oxide nanoclusters (SnO2-rGO) as electrochemical sensing material for H2O2 detection. From scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HRTEM) images, uniform SnO2 nanoclusters with a diameter of 3–5 nm are evenly dispersed on the surface of rGO. Electrochemical studies showed that the sensing platform fabricated from SnO2-rGO possesses fast mass transport, good electrical conductivity and high sensitivity and selectivity for the detection of H2O2. The SnO2-rGO composite exhibited a linear current response to H2O2 from 0.5 to 800 μM with a fast response within 2 s. The detection limit was calculated to be 0.478 μM. The present study shows that tiny SnO2 clusters supported on rGO can be applied as a promising type of sensing material for electrochemical detection of H2O2.
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