Effects of fabrication parameters on the mechanical properties of short basalt‐fiber‐reinforced thermoplastic composites for fused deposition modeling‐based 3D printing

材料科学 复合材料 极限抗拉强度 熔融沉积模型 复合数 玄武岩纤维 纤维 热重分析 挤压 制作 3D打印 医学 病理 有机化学 化学 替代医学
作者
Luqing Hua,Xin Wang,Ding Li,Siheng Zeng,Jianxun Liu,Zhishen Wu
出处
期刊:Polymer Composites [Wiley]
卷期号:44 (6): 3341-3357 被引量:3
标识
DOI:10.1002/pc.27325
摘要

Abstract This study develops sustainable and recyclable basalt fiber (BF)‐reinforced flexible plastic low‐temperature polyamide (L‐PA) filaments for fused deposition modeling (FDM)‐3D printing and optimizes fabrication parameters to achieve eco‐friendliness, high mechanical performance, and lightweight FDM‐fabricated composite parts. Herein, 15 wt% fiber‐filled composite filaments were prepared by an extrusion process. Three manufacturing parameters, including printing temperature, printing speed, and layer height, were investigated for their effects on the tensile and compression properties through Taguchi L9 orthogonal experiments. To obtain a suitable printing temperature range, the thermal behaviors of the composite filaments were characterized by differential scanning calorimetry, thermogravimetric analysis, and melt flow factor measurements. In addition, the FDM‐printed specimen surface and tensile fracture interface after tensile tests were observed and analyzed by SEM. Results show that the printing temperature has the greatest effect on the mechanical properties of the BF/L‐PA composites, followed by the layer height, whereas the printing speed has the least effect. This indicates that better mechanical properties can be obtained at higher printing temperatures and lower layer heights. Compared with neat L‐PA, adding BF to L‐PA improves the tensile modulus, tensile strength, and specific energy absorption per volume without sacrificing ductility, showing the maximal increases of 176.6%, 142.0%, and 172.2%, respectively, as compared with neat L‐PA. A SEM micrograph reveals that the primary factors for these improvements are the fibers acting as reinforcement filling in the L‐PA matrix and the good bonding properties between the adjacent infills in a single layer and among successive layers.
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