三七
色谱法
化学
气相色谱法
再现性
毛细管气相色谱法
残余物
毛细管作用
材料科学
数学
算法
医学
病理
复合材料
替代医学
作者
Hanhua Wang,Zhen-zhen Ni,Tong-Wei Yao
出处
期刊:PubMed
日期:2007-11-01
卷期号:36 (6): 598-603
标识
DOI:10.3785/j.issn.1008-9292.2007.06.014
摘要
To develop a headspace gas chromatography method for the determination of residual organic solvents in Panax notoginseng extracts.The samples were injected into HP-INNOWAX capillary column by headspace sampler and analyzed with FID detector using standard addition method.There was a good linearity in the experimental concentration (r=0.9932-0.9999). The rate of recovery was in the rang of 81.74%-111.2%. The numbers of theoretical plates were more than 15000 and the resolutions between the adjacent peaks were more than 2. The RSD of precision and accuracy were both less than 10 %.The method is simple,accurate and sensitive with good reproducibility, which can be used for the determination of the residual organic solvents in Panax notoginseng extracts.
科研通智能强力驱动
Strongly Powered by AbleSci AI