麦芽糊精
喷雾干燥
化学
傅里叶变换红外光谱
食品科学
扫描电子显微镜
玻璃化转变
产量(工程)
水活度
化学工程
差示扫描量热法
无定形固体
含水量
材料科学
色谱法
有机化学
复合材料
聚合物
热力学
物理
工程类
岩土工程
作者
Liangqing Zhang,Xianhai Zeng,Nan Fu,Xing Tang,Yong Sun,Lu Lin
标识
DOI:10.1016/j.foodres.2018.01.004
摘要
The aim of this study was to evaluate the influence of spray-drying on the powder qualities and microstructures of prebiotic xylooligosaccharides (XOS). The relationships between glass transition temperature (Tg) and XOS retention, moisture content, drying yield as well as specific surface area under different inlet air temperatures and maltodextrin concentrations were investigated. Antioxidant activity retention, hygroscopicity, color attributes, X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR) of the spray-dried XOS product were also assessed. The results indicated that an increase in inlet air temperature decreased the moisture content, hence the Tg value was increased. Higher maltodextrin concentration increased the Tg value, and was attributed to the molecular weight increase. The wall deposition was a tendency to occur when the temperature beyond the Tg, reduced the drying yield. Higher temperature and wall deposition promoted the decomposition of XOS into monosaccharide. The crust formation rate of droplets and stickiness of microparticles were affected by Tg, and hence, influenced the specific surface area. The antioxidant activity retention of XOS exhibited a concentration-dependent behavior. The hygroscopicity of the microparticles could be reduced by both of the low inlet air temperature and high maltodextrin concentration. According to the results of color attributes, XRD and SEM, the particles were colorless and amorphous, and tended to become more spherical and scattered with the addition of maltodextrin. The FT-IR analysis confirmed that no chemical reaction occurred between XOS and agent, which indicated that maltodextrin is a promising carrier for producing bioactive XOS powder.
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