纳米棒
黄铁矿
拉曼光谱
热液循环
高分辨率透射电子显微镜
光催化
X射线光电子能谱
棒
产量(工程)
再现性
水热合成
材料科学
化学
纳米技术
化学工程
矿物学
分析化学(期刊)
催化作用
光学
复合材料
透射电子显微镜
冶金
色谱法
有机化学
工程类
医学
替代医学
物理
病理
作者
M.V. Morales-Gallardo,A. Ayala,Mou Pal,M.A. Cortés-Jácome,J.A. Toledo-Antonio,N.R. Mathews
标识
DOI:10.1016/j.cplett.2016.07.046
摘要
Abstract In this work, FeS2 nanorods were synthetized by hydrothermal method. The advantages of our process were the high yield, simplicity and reproducibility. The material was studied in detail using different experimental tools such as XRD, SEM, HRTEM, EDXS, XPS, Raman, and UV–vis reflectance. XRD pattern and Raman data revealed good crystalline quality for the as synthesized pyrite FeS2. SEM analysis displayed the rod-like morphologies of FeS2 which seemed to grow radially from a center giving a flower-like appearance. From TEM images the approximate length and diameter of nano-rods were determined as 275 and 15 nm respectively. The material showed excellent photocatalytic activity which was assessed from the degradation of the methlyene blue.
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