选区衍射
X射线光电子能谱
纳米线
材料科学
扫描电子显微镜
透射电子显微镜
模板方法模式
钙钛矿(结构)
化学工程
氧化物
溶胶凝胶
结晶学
纳米技术
化学
复合材料
冶金
工程类
作者
Yang Liu,Yi Huang,Bin Dong,Hu‐Lin Li
标识
DOI:10.1016/j.jssc.2005.01.022
摘要
The highly ordered LaNiO3 nanowires of the rare-earth perovskite-type composite oxide were controlled synthesized within a porous anodic aluminum oxide (AAO) template by means of sol–gel method using nitrate as raw materials and citric acid as chelating agent. The results of scanning electron microscopy (SEM) and transmission electron microscopy (TEM) revealed that the obtained LaNiO3 nanowires had a uniform length and diameter, which were determined by the thickness and the pore diameter of the applied AAO template. The results of X-ray diffraction (XRD) and the selected-area electron diffraction (SAED) indicated that the LaNiO3 nanowires were perovskite-type crystalline structures. Furthermore, X-ray photoelectron spectroscopy (XPS) and the energy dispersive X-ray (EDX) spectroscopy demonstrated that the stoichiometric LaNiO3 was formed.
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