It was desired to determine the distribution of boron in the various steps of the processing of domestic ore concentrates containing high percentages of boron. The experiments described in this report were directed toward that end. Summary of this report are: (1) a black oxide containing 0.6 ppm of boron was prepared from material containing 350 ppm; (2) less than 0.02% of the boron in the original material appeared in the black oxide; (3) the iron step did not remove appreciable amounts of boron; (4) the bulk of the extracted boron was removed in the soda salt precipitation; and (5) some of the boron was removed in the acid leach and calcination steps.