精炼(冶金)
杂质
区域熔化
钛
材料科学
钛合金
氮气
碳纤维
压痕硬度
冶金
分析化学(期刊)
氧气
微观结构
复合材料
化学
合金
色谱法
有机化学
复合数
作者
O.E. Kozhevnikov,М.М. Pylypenko,A. P. Shcherban,О.А. Datsenko,V.M. Pelykh,V.D. Virych
标识
DOI:10.46813/2021-135-070
摘要
The physical substantiation of titanium refining by crucibleless electron beam zone melting (ZM) method in vacuum was presented. Calculations of the equilibrium, limiting and effective distribution coefficients for impurity elements in the base metal were carried out. The refining of titanium was studied experimentally, and samples with a purity of 99.92 wt.% were received. The total content of impurities was reduced by a factor of 1.5 (from 0.12 to 0.08 wt.%). The concentration of interstitial impurities was significantly reduced (oxygen – by 1.3; carbon – by 2; nitrogen – by 2.5 times). The structure and microhardness were investigated.
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