选区衍射
傅里叶变换红外光谱
纳米颗粒
透射电子显微镜
光致发光
材料科学
扫描电子显微镜
吸收光谱法
分析化学(期刊)
吸收(声学)
光谱学
粒径
核化学
纳米技术
化学工程
化学
光学
物理化学
有机化学
光电子学
物理
工程类
复合材料
量子力学
摘要
The development of green synthesis route through biological method for the synthesis of nanoparticles using plants have received attention in the recent times as it is environment friendly and economical method. ZnS nanoparticles have been prepared using glucose both as capping agent and stabilizer. The obtained ZnS nanoparticles are studied by X-ray diffraction (XRD), Energy dispersive analysis of X-rays (EDAX), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Selected area electron diffraction (SAED), UV-vis optical absorption, Photoluminescence techniques (PL) and Fourier Transform Infrared Spectroscopy (FTIR). The mean particle size of the ZnS nanoparticles is found to be 5.8 nm. The XRD analysis confirms the cubic and crystalline nature of the synthesized sample which is in good agreement with SAED pattern. Also, EDAX pattern confirms the presence of Zinc and Sulfur. . UV-vis spectra show that the absorption peaks exhibit blue shift from the bulk. The PL investigation revealed the recombination mechanism in ZnS nanoparticles. FTIR spectra confirm the presence of glucose as capping agent.
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