材料科学
微乳液
正交晶系
纳米颗粒
光致发光
扫描电子显微镜
傅里叶变换红外光谱
光谱学
透射电子显微镜
吸收光谱法
钙钛矿(结构)
化学工程
镧
场发射显微术
分析化学(期刊)
晶体结构
纳米技术
无机化学
结晶学
衍射
化学
有机化学
光学
光电子学
肺表面活性物质
复合材料
物理
工程类
量子力学
作者
Reza Abazari,Soheila Sanati
标识
DOI:10.1016/j.spmi.2013.09.017
摘要
Orthorhombic structure of lanthanum ferrite nanoparticles (LaFeO3 NPs) with perovskite type phase has been synthesized with water-in-oil (W/O) microemulsion consisted of water/dioctyl sulfosuccinate sodium (aerosol-OT)/isooctane at room temperature. It has been shown that aerosol-OT reverse microemulsion solution is appropriate for synthesizing perovskite LaFeO3 NPs in the absence of any co-surfactants. Field emission scanning electron microscope (FE-SEM), transmission electron microscopy (TEM), energy dispersive analysis of X-ray (EDAX), X-ray diffraction (XRD), ultraviolet–visible absorption spectroscopy (UV–Vis), and Fourier transform infrared spectroscopy (FT-IR) have been adopted for characterization of surface morphology, size, phase composition, structure, and optical properties of the considered NPs. Furthermore, the optical properties of LaFeO3 NPs have been further analyzed via photoluminescence (PL) spectroscopy. As shown by the physicochemical characterizations, our prepared NPs via aerosol-OT reverse microemulsion solution are spherical and nearly uniform (with a size of about 24.65 nm). Besides, they include an orthorhombic phase while no impurities are observed. Single phase lanthanum ferrite NPs have successfully been prepared at 500 °C. Moreover, UV–Vis spectrum indicates that the LaFeO3 NPs synthesized through this technique can be considered as a type of photo-catalytic materials.
科研通智能强力驱动
Strongly Powered by AbleSci AI