电合成
电化学
化学
组合化学
纳米技术
电解质
基质(水族馆)
材料科学
电极
物理化学
海洋学
地质学
作者
Mingyu Zhang,Zhaochu Luo,Xinye Tang,Ling Yu,Junchen Pei,Junlei Wang,Caicai Lu,Binbin Huang
摘要
An efficient electrochemical selenocyclization strategy for the synthesis of 3-selenylindoles from 2-ethynylanilines and diselenides has been developed in simple tube- or beaker-type undivided cells under ambient conditions. Notably, these sustainable transformations are completed within a short time with low equivalents of charges, diselenides and electrolytes, exhibiting a broad substrate scope with excellent functional group compatibility. Moreover, a gram-scale electrosynthesis and late-stage functionalization of complex molecules further demonstrate the practical synthetic potential of this facile electrochemical system.
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