材料科学
放电等离子烧结
碳化钨
压痕硬度
田口方法
碳化硅
烧结
维氏硬度试验
复合材料
钨
氮化硅
冶金
硅
微观结构
作者
Sultan Althahban,P. Gurusamy,Faez Qahtani,Yosef Jazaa,Saeed Mousa,Sanipina Anjani Devi,Melvin Victor De Poures,Ram Subbiah,Hana Beyene Mamo
摘要
It is usual practice to optimize the various processing parameters in order to achieve well-organized and lucrative process conditions. For the creation of tungsten carbide/silicon nitride/AA2219 composites, sintering temperature, sintering pressure, dwelling time, and heating rate all must be optimized. Design of experiments and analysis of variance were employed to assess the factors’ contributions to density as well as microhardness response variables. It was decided to test the admixed powders and Vickers hardness tester, optical microscope, and Archimedes-based density testing to evaluate the sintered compacts. The optimum spark plasma sintering factors were a temperature of 500°C, a pressure of 30 MPa, a dwelling time of 8 minutes, and a heat rate of 160 °C/min, resulting in an extreme density of 2.71 g/cm3 and a maximum microhardness of 38.61 HV (0.38 GPa).
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