Results are reported on the study and quantitative determination of berkelium by the coulometric method in 1 M sulfuric acid, in solutions of nitric acid, and in mixtures of these acids. The best results in the determination of berkelium were obtained in solutions of a mixture of nitric and sulfuric acids. In 1 M HNO/sub 3/ + 0.1 M H/sub 2/SO/sub 4/ solutions, berkelium can be determined with an accuracy within approx. +/- 2%, when its content is 10 ..mu..g/ml.