吸气剂
材料科学
钛
钯
扫描电子显微镜
氧气
透射电子显微镜
薄膜
分析化学(期刊)
复合材料
冶金
化学
纳米技术
光电子学
催化作用
色谱法
有机化学
生物化学
作者
Yuta Sato,Takashi Kikuchi,Tetsuya Miyazawa,S. Ohno,Ayako Hashimoto,Misao Yamanaka,Kazuhiko Mase
出处
期刊:Vacuum
[Elsevier BV]
日期:2023-03-15
卷期号:212: 112004-112004
标识
DOI:10.1016/j.vacuum.2023.112004
摘要
A zero-length conflat fin-type nonevaporable getter (NEG) pump deposited with oxygen-free palladium/titanium (Pd/Ti) has been developed. The NEG pump was activated by baking and its pumping speeds were measured as a function of baking time and baking temperature. The NEG pump can be fully activated by baking at 150 °C for 12 h and exhibits initial pumping speeds of 2340 L s−1 for H2, and 1440 L s−1 for CO. The initial pumping speeds of the oxygen-free Pd/Ti thin film after baking at 150 °C were estimated to be 3.2 L s−1 cm−2 for H2 and 7.6 L s−1 cm−2 for CO. The morphologies of oxygen-free Pd/Ti thin films on the partition plates and the bottom were examined by scanning electron microscopy, scanning transmission electron microscopy, and energy-dispersive X-ray spectroscopy. The Ti thin film was completely coated with Pd on the bottom, whereas the partition plates were covered by Pd/Ti nanostructures. The present NEG pump is ideal for maintaining ultrahigh vacuum below 10−8 Pa, because its pumping speeds for H2 and CO are quite large, and because it can be fully activated by baking at 150 °C for 12 h.
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