Synthesis of some unsymmetrically deuterated cyclohexanols

Abstract The preparations of [1,2,2,3,3,6,6‐D7]Cyclohexanol, and of two isotopameric [1,2,2,3,4,5,5,6,6‐D9]Cyclohexanols are described. The isotopic purity of the deuterium labeled cyclohexanols is better than 90 %.